Experimental analysis of wear resistance of compacts of fine-dispersed iron powder and tungsten monocarbide nanopowder produced by impulse pressing

The paper presents the results of studying the structure and wear resistance of compacts produced from fine dispersed reduced iron powder (average particle size 3–5μm) with the addition of tungsten carbide (WC) nanopowder with the average particle size of 25–30 nm. The mass fraction of tungsten carbide (wolfram carbide) in the powder composition was 5% and 10% of the total mass. Impulse pressing was conducted using the modified Kolsky method at compacting temperatures of 20 °C to 300 °C. The produced compacts had relative density of over 90%. Metallographic studies using the scanning electronic microscopy method on a TESCAN VEGA II electronic microscope have shown that the produced compacts have a fairly homogeneous fine-grained structure, with a uniform pattern of pore distribution, the form of the pores being close to spherical. X-ray microanalysis using an INCA Energy 250 energy-dispersion spectrometer with scanning along the surface line and transversal laps testifies to the fact that, in the considered temperature range, dynamic compaction does not lead to any noticeable changes in the distribution of the Fe, W and C elements over the bulk of the specimens. The conducted measurements of micro-hardness of the compacts have shown that it increases considerably with the pressing temperature. The produced compacts were tested for wear resistance in a dry friction regime, using the ‘rotating disk – stationary specimen’ configuration. Mass loss of the compacts as a function of testing time is presented. Wear resistance of compacts depends on pressing temperature and concentration of the WC powder in the matrix of reduced iron. It has been experimentally determined that maximal wear resistance is observed in the compacts with the mass fraction of WC equal to 10%, produced at a pressing temperature of 300 °C.