N,N′-dibutyloxamide (1) was prepared by reacting diethyloxalate with n-butylamine in ethyl alcohol and characterized by microanalytical techniques, FT-IR, and NMR spectroscopy. Crystals suitable for single crystal X-ray diffraction (SC-XRD) were obtained from an acetonitrile solution of 1, and the structural characterization showed the presence of intermolecular hydrogen bonding interactions.
N,N′-Dibutyloxamide
Enrico Podda;Massimiliano Arca;M. Carla Aragoni;Vito Lippolis;Anna Pintus
2023-01-01
Abstract
N,N′-dibutyloxamide (1) was prepared by reacting diethyloxalate with n-butylamine in ethyl alcohol and characterized by microanalytical techniques, FT-IR, and NMR spectroscopy. Crystals suitable for single crystal X-ray diffraction (SC-XRD) were obtained from an acetonitrile solution of 1, and the structural characterization showed the presence of intermolecular hydrogen bonding interactions.
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