4,4 '-(Disulfanediyl)dipyridinium chloride triiodide, C10H10N2S22+center dot Cl-center dot I-3(-), (1) was synthesized by reaction of 4,4 '-dipyridyldisulfide with ICl in a 1:1 molar ratio in dichloromethane solution. The structural characterization of 1 by SC-XRD analysis was supported by elemental analysis, FT-IR, and FT-Raman spectroscopic measurements.

Crystal structure of 4,4′-(disulfanediyl)dipyridinium chloride triiodide

Podda, Enrico;Aragoni, M. Carla;Caltagirone, Claudia;De Filippo, Greta;Garau, Alessandra;Lippolis, Vito;Pintus, Anna;Arca, Massimiliano
2024-01-01

Abstract

4,4 '-(Disulfanediyl)dipyridinium chloride triiodide, C10H10N2S22+center dot Cl-center dot I-3(-), (1) was synthesized by reaction of 4,4 '-dipyridyldisulfide with ICl in a 1:1 molar ratio in dichloromethane solution. The structural characterization of 1 by SC-XRD analysis was supported by elemental analysis, FT-IR, and FT-Raman spectroscopic measurements.
2024
SC-XRD
bis­(pyridine-4-yl)di­sulfide
crystal structure
halogen bonding
polypyridyl donors
polyhalides
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Utilizza questo identificativo per citare o creare un link a questo documento: https://hdl.handle.net/11584/416523
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